DS DS/EN 16159
DS DSEN 16159 2012-MAR-07 Anmal feedng stuffs - Determnaton of selenum by hydrde generaton atomc absorpton spectrometry HGAAS after mcrowave dgeston dgeston wth 65 ntrc acd and 30 hydrogen peroxde
DS DSEN 16159 2012-MAR-07 Anmal feedng stuffs - Determnaton of selenum by hydrde generaton atomc absorpton spectrometry HGAAS after mcrowave dgeston dgeston wth 65 ntrc acd and 30 hydrogen peroxde
This European Standard specifies a method for the determination of selenium in animal feeding stuffs by hydride generation atomic absorption spectrometry (HGAAS) after microwave pressure digestion. The method was successfully tested by an inter-laboratory study of CEN/TC 327/WG 4 in the range of 0,25 mg/kg to 74 mg/kg. The limit of quantification is 0,5 µg/l of the test solution which corresponds to the calibration standard 2. Using a test portion of 0,5 g and a volume of the test solution of 25 ml after pressure digestion the limit of quantification is calculated as 0,125 mg/kg in the feed material. NOTE A lower limit of quantification could be achieved - each laboratory has to prove it.